- heat / boil the filtrate
- until crystals form in a cooled sample / on a glass rod
- leave the solution to cool / crystallise
- filter to remove the crystals
- dry the crystals on filter paper / paper towel / in a warm oven / in a desiccator / leave to dry
Accept:
- heat to crystallisation point / form a saturated solution / until crystals start to form / remove some of the water
- decant the excess solution
Reject:
- hot oven or direct heating, e.g. Bunsen burner, for drying
Marking guidance:
- If the solution is heated to remove all the water, only the heating mark can be awarded.
- If the solution is left to evaporate all the water without heating, only 1 mark can be awarded.
- Crystallisation-point mark depends on heating.
- If the solution is left to completely evaporate after heating, award max 3.
- No drying mark if crystals are washed after drying.