Edexcel IGCSE Chemistry Experimental Skills
Practise Edexcel IGCSE Chemistry experimental skills by improving methods, choosing apparatus, increasing accuracy and testing deductions.
- Syllabus
- Issue 3 (2024)
- Course
- Chemistry 4CH1
Practise Edexcel IGCSE Chemistry experimental skills by improving methods, choosing apparatus, increasing accuracy and testing deductions.
A student uses this apparatus to investigate the effect of heat on different solid metal carbonates.

This is the student's method.
- use a spatula to put some metal carbonate in the boiling tube
- fit the delivery tube into position
- pour some limewater into the test tube
- start a timer and immediately begin to heat the metal carbonate
- record the time when a change first occurs in the limewater
The student repeats the method using different metal carbonates.
When a metal carbonate is heated a reaction sometimes occurs.
The equation for the reaction is
State two variables that the student should control in this investigation.
1
2
any two of the following:
M4 (use same) size flame / distance of flame from boiling tube OWTTE
ALLOW mass
Suggest why bubbles appear in the limewater immediately after heating has started but before there is any change to the metal carbonate.
bubbles are air (from tube) / caused by air (expanding on heating)
ALLOW gas in tube expands (on heating)
State how you should extend the investigation to see if your deduction is correct.
repeat (the investigation) using different / other / more
(metal) carbonates
A student uses this apparatus to investigate the rate of reaction between dilute sulfuric acid and an excess of small pieces of zinc.

This is the student's method.
Step 1 use 50 cm3 of dilute sulfuric acid
Step 2 add approximately 5 g of small zinc pieces to the sulfuric acid
Step 3 quickly connect the gas syringe
Step 4 record the reading on the gas syringe every 30 seconds until the reaction stops
Name a suitable piece of apparatus to measure the volume of sulfuric acid.
measuring cylinder
ALLOW burette / pipette / syringe
REJECT gas syringe
Give a reason why the mass of zinc pieces does not need to be measured accurately.
(the) zinc / Zn / it is in excess
Give a reason why the student quickly connects the gas syringe in step 3.
so as little gas as possible is lost
ACCEPT to keep as
much gas as possible
State how the student would know when the reaction stops.
any one from
no further effervescence / bubbles / fizzing
no more gas collects in the syringe
ALLOW gas syringe does not move
A student investigates the effect of temperature on the rate of reaction between two solutions, A and B . When the reaction occurs, the mixture turns from colourless to blue.
This is the student's method.
- pour 25 cm3 of solution A into a conical flask
- add solution B and measure the temperature of the mixture
- record the time taken for the mixture to turn blue
The student repeats this method at different temperatures.
Give two variables that the student needs to keep constant in this investigation.
1
2
Any two from
M1 concentration of solution A
M2 concentration of solution B
M3 volume of solution B
ALLOW amount of solution B
Ignore apparatus
The table shows the student's results.

Draw a circle around the anomalous result.
anomalous point at 25∘C circled
ALLOW ecf from
incorrect plotting
Give a reason for the anomalous result.
Any one from
M1 temperature was higher than 25∘C
M2 started the timer too late / stopped the timer too early/took reading too early
ALLOW ecf from
incorrect anomalous
result circled so