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CAIE IGCSE Chemistry Practical and Chemical Analysis Questions

Practise laboratory apparatus, separation, titration, chromatography and qualitative tests across the CAIE IGCSE Chemistry experimental techniques unit.

Syllabus
2026–2028
Course
Chemistry 0620

12. Experimental techniques and chemical analysis question 1

[Maximum number: 3]

Sulfur is an important element.

Question (a)

(a)

Dilute sulfuric acid is used to make salts known as sulfates.

A method consisting of three steps is used to make zinc sulfate from zinc carbonate.
step 1 Add an excess of zinc carbonate to 20 cm320 \mathrm{~cm}^{3} of 0.4 mol/dm30.4 \mathrm{~mol} / \mathrm{dm}^{3} dilute sulfuric acid until the reaction is complete.
step 2 Filter the mixture.
step 3 Heat the filtrate until a saturated solution forms and then allow it to crystallise.

[ 3 ]

Question (i)

(i)

Name a suitable piece of apparatus for measuring 20 cm320 \mathrm{~cm}^{3} of dilute sulfuric acid in step 1.

[ 1 ]

Question (ii)

(ii)

What is meant by the term saturated solution in step 3?

[ 2 ]

12. Experimental techniques and chemical analysis question 2

[Maximum number: 4]

Question (a)

(a)

Dilute sulfuric acid and aqueous sodium hydroxide can be used to prepare sodium sulfate crystals using a method that involves titration.

Figure for Question (a) — CAIE IGCSE Chemistry
[ 2 ]

Question (i)

(i)

Suggest why universal indicator is not suitable for this titration.

[ 1 ]

Question (ii)

(ii)

Name an indicator that can be used in this titration.
20.0 cm320.0 \mathrm{~cm}^{3} of dilute sulfuric acid neutralises 25.0 cm325.0 \mathrm{~cm}^{3} of 1.00 mol/dm31.00 \mathrm{~mol} / \mathrm{dm}^{3} aqueous sodium hydroxide. At the end of the titration the conical flask contains aqueous sodium sulfate with the dissolved indicator as an impurity.

[ 1 ]

Question (b)

(b)

Sodium hydrogensulfate, NaHSO4\mathrm{NaHSO}_{4}, dissolves in water to produce an aqueous solution, X, containing Na+,H+\mathrm{Na}^{+}, \mathrm{H}^{+}and SO42\mathrm{SO}_{4}{ }^{2-} ions.

State the observations when the following tests are done.

[ 2 ]

Question (i)

(i)

A flame test is carried out on X.

[ 1 ]

Question (ii)

(ii)

Acidified aqueous barium nitrate is added to X.

[ 1 ]

12. Experimental techniques and chemical analysis question 3

[Maximum number: 4]

Name the process used to:

Question (a)

(a)

separate an insoluble solid from a mixture of an insoluble solid and a solution

[ 1 ]

Question (b)

(b)

identify the components of a mixture of soluble coloured substances

[ 1 ]

Question (c)

(c)

separate a mixture of several liquids with different boiling points

[ 1 ]

Question (d)

(d)

determine the volume of an acid required to neutralise a given volume of an alkali.

[ 1 ]

12. Experimental techniques and chemical analysis question 4

[Maximum number: 3]

The chemical equation for the complete combustion of ethanol, C2H5OH\mathrm{C}_{2} \mathrm{H}_{5} \mathrm{OH}, is shown.

C2H5OH+3O22CO2+3H2O\mathrm{C}_{2} \mathrm{H}_{5} \mathrm{OH}+3 \mathrm{O}_{2} \rightarrow 2 \mathrm{CO}_{2}+3 \mathrm{H}_{2} \mathrm{O}

The energy released when one mole of ethanol undergoes complete combustion is 1280 kJ .
Part of the energy level diagram for this reaction is shown.

Figure for Question 12. Experimental techniques and chemical analysis question 4 — CAIE IGCSE Chemistry

Question (a)

(a)

Dodecane is an alkane containing 12 carbon atoms. Ethanol can be manufactured from dodecane in a two-stage process.

In stage 1, each molecule of dodecane is converted into three molecules of ethene and one molecule of another hydrocarbon.

[ 2 ]

Question (i)

(i)

Suggest how to test the purity of the ethanol produced.

[ 2 ]

Question (b)

(b)

Ethanol can also be manufactured by the fermentation of glucose, C6H12O6\mathrm{C}_{6} \mathrm{H}_{12} \mathrm{O}_{6}.

[ 1 ]

Question (i)

(i)

Suggest the name of a process to obtain ethanol from a mixture of ethanol and water.

[ 1 ]
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